Method note us epa 3015a aqueous sample mars 6 ramp times and power may vary depending on the type and number of vessels. Microwave assisted acid digestion of aqueous samples and extracts. Microwave assisted acid digestion of aqueous samples and extracts, part of test methods for evaluating solid waste, physicalchemical methods pdf 25 pp, 168 k, february 2007 contact us to ask a question, provide feedback, or report a problem. You may need a pdf reader to view some of the files on this page. Therefore, method procedures are written based on the assumption that they will be performed by analysts who are. A representative aqueous sample is extracted with concentrated nitric acid or, optionally, concentrated nitric acid and concentrated hydrochloric acid, using microwave heating with a suitable. Analytes for which epa has demonstrated the acceptability of this method in a.
Microwave digestion of method note us epa 3015a aqueous. A representative aqueous sample is extracted with concentrated nitric acid or, optionally, concentrated nitric acid and concentrated hydrochloric acid, using microwave heating with a suitable laboratory microwave unit. This document explains the acid extractiondissolution method for metals in aqueous samples, drinking water, mobilityprocedure extracts, and wastes that contain suspended solids. Sw846 is not intended to be an analytical training. Method type one touch control type standard control sample type water heating program max sample weight 45 ml reagents hno. Since this method is not intended to accomplish total decomposition of the sample, the extracted analyte concentrations may not reflect the total content in the sample. Epa 8000 series method the epa 8000 methods are designed for monitoring organic pollutants in ground water, as prescribed in the resource recovery and conservation act rcra. The information contained in this method is provided by epa as guidance to be. View actual epa method 3015a pdf file epa method 3015a. Microwave assisted acid digestion of aqueous samples and extracts summary. Hcl optional recommended vessels easyprep plus marsxpress marsxpress plus recommended equipment mars 6. The option to add hcl in addition to hno3 provides better complexation and recovery of certain metals that are regulated by the resource conservation and recovery act rcra than the original hno3only method 3015. Microwave digestion of method note us epa 3015 aqueous.
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